Information card for entry 4073287

Structure parameters

• Formula: C23 H54 O11 P3 Re Sn
• Calculated formula: C23 H54 O11 P3 Re Sn
• SMILES: [Re]([Sn](C)(C)C)([P](OCC)(OCC)OCC)([P](OCC)(OCC)OCC)([P](OCC)(OCC)OCC)(C#[O])C#[O]
• Title of publication: Preparation and Reactivity of Stannyl Complexes of Manganese and Rhenium
• Authors of publication: Albertin, Gabriele; Antoniutti, Stefano; Castro, Jesús; García-Fontán, Soledad; Zanardo, Gianluigi
• Journal of publication: Organometallics
• Year of publication: 2007
• Journal volume: 26
• Journal issue: 11
• Pages of publication: 2918
• a: 28.12 ± 0.002 Å
• b: 10.7089 ± 0.0009 Å
• c: 30.4873 ± 0.0017 Å
• α: 90°
• β: 122.795 ± 0.005°
• γ: 90°
• Cell volume: 7717.5 ± 1 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.2602
• Residual factor for significantly intense reflections: 0.056
• Weighted residual factors for significantly intense reflections: 0.0862
• Weighted residual factors for all reflections included in the refinement: 0.1198
• Goodness-of-fit parameter for all reflections included in the refinement: 0.75
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No