Crystallography Open Database

Information card for entry 4073288

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Coordinates	4073288.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C22 H48 O16 P3 Re Sn
Calculated formula	C22 H48 O16 P3 Re Sn
Title of publication	Preparation and Reactivity of Stannyl Complexes of Manganese and Rhenium
Authors of publication	Albertin, Gabriele; Antoniutti, Stefano; Castro, Jesús; García-Fontán, Soledad; Zanardo, Gianluigi
Journal of publication	Organometallics
Year of publication	2007
Journal volume	26
Journal issue	11
Pages of publication	2918
a	11.1114 ± 0.0011 Å
b	11.951 ± 0.0013 Å
c	16.5529 ± 0.0017 Å
α	109.711 ± 0.002°
β	92.817 ± 0.002°
γ	114.348 ± 0.002°
Cell volume	1839.3 ± 0.3 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0684
Residual factor for significantly intense reflections	0.0459
Weighted residual factors for significantly intense reflections	0.09
Weighted residual factors for all reflections included in the refinement	0.0965
Goodness-of-fit parameter for all reflections included in the refinement	0.897
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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