Information card for entry 4073389

Structure parameters

• Formula: C51.5 H48 Sn V4
• Calculated formula: C49.75 H44 Sn V4
• Title of publication: Tetrakis([5]trovacenyl)tin: Synthesis, Structure, and Intramolecular Communication†
• Authors of publication: Elschenbroich, Christoph; Lu, Feng; Nowotny, Mathias; Burghaus, Olaf; Pietzonka, Clemens; Harms, Klaus
• Journal of publication: Organometallics
• Year of publication: 2007
• Journal volume: 26
• Journal issue: 16
• Pages of publication: 4025
• a: 13.7723 ± 0.0006 Å
• b: 16.9996 ± 0.0007 Å
• c: 18.7871 ± 0.0008 Å
• α: 83.322 ± 0.003°
• β: 69.348 ± 0.003°
• γ: 78.093 ± 0.003°
• Cell volume: 4022.7 ± 0.3 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0395
• Residual factor for significantly intense reflections: 0.0268
• Weighted residual factors for significantly intense reflections: 0.0629
• Weighted residual factors for all reflections included in the refinement: 0.0657
• Goodness-of-fit parameter for all reflections included in the refinement: 0.975
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No