Information card for entry 4073510

Structure parameters

• Common name: 04168
• Formula: C13 H29 Cs O Si2
• Calculated formula: C13 H29 Cs O Si2
• Title of publication: Trimethylsilylated Allyl Complexes of the Heavy Alkali Metals, M[1,3-(SiMe3)2C3H3](thf)n(M = K, Cs)
• Authors of publication: Quisenberry, Keith T.; Gren, Cameron K.; White, Rosemary E.; Hanusa, Timothy P.; Brennessel, William W.
• Journal of publication: Organometallics
• Year of publication: 2007
• Journal volume: 26
• Journal issue: 17
• Pages of publication: 4354
• a: 6.4496 ± 0.0008 Å
• b: 10.1112 ± 0.0013 Å
• c: 30.041 ± 0.004 Å
• α: 90°
• β: 90.587 ± 0.002°
• γ: 90°
• Cell volume: 1959 ± 0.4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0672
• Residual factor for significantly intense reflections: 0.0574
• Weighted residual factors for significantly intense reflections: 0.1161
• Weighted residual factors for all reflections included in the refinement: 0.1198
• Goodness-of-fit parameter for all reflections included in the refinement: 1.043
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No