Crystallography Open Database

Information card for entry 4073511

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Coordinates	4073511.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	2b
Formula	C39 H76 O P Rh Si6
Calculated formula	C39 H76 O P Rh Si6
Title of publication	Synthesis and Properties of a Rhodium Complex Having a Novel β-Ketophosphenato Ligand, a Heavier Congener of a β-Ketoiminato Ligand#
Authors of publication	Sasamori, Takahiro; Matsumoto, Teruyuki; Takeda, Nobuhiro; Tokitoh, Norihiro
Journal of publication	Organometallics
Year of publication	2007
Journal volume	26
Journal issue	15
Pages of publication	3621
a	10.0909 ± 0.0002 Å
b	11.1677 ± 0.0002 Å
c	22.256 ± 0.0004 Å
α	102.312 ± 0.0013°
β	90.6913 ± 0.0008°
γ	104.418 ± 0.001°
Cell volume	2367.57 ± 0.08 Å³
Cell temperature	103 ± 2 K
Ambient diffraction temperature	103 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0441
Residual factor for significantly intense reflections	0.0396
Weighted residual factors for significantly intense reflections	0.0926
Weighted residual factors for all reflections included in the refinement	0.095
Goodness-of-fit parameter for all reflections included in the refinement	1.107
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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