Information card for entry 4073527

Structure parameters

• Common name: organotinphosphate
• Formula: C46 H60 O12 P2 Sn3
• Calculated formula: C46 H59 O12 P2 Sn3
• Title of publication: Formation of a Double-Bicapped Hexatin Phosphate Cage by a De-arylation Reaction. Synthesis and Structure of [(PhSn)6(μ-OH)2(μ3-O)2(μ-OEt)4{(ArO)PO3}4] (Ar = 2,6-i-Pr2C6H3)
• Authors of publication: Chandrasekhar, Vadapalli; Sasikumar, Palani; Thilagar, Pakkirisamy
• Journal of publication: Organometallics
• Year of publication: 2007
• Journal volume: 26
• Journal issue: 18
• Pages of publication: 4386
• a: 15.913 ± 0.005 Å
• b: 16.52 ± 0.005 Å
• c: 19.837 ± 0.005 Å
• α: 90 ± 0.005°
• β: 95.946 ± 0.005°
• γ: 90 ± 0.005°
• Cell volume: 5187 ± 3 ų
• Cell temperature: 273 ± 2 K
• Ambient diffraction temperature: 273 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0705
• Residual factor for significantly intense reflections: 0.0512
• Weighted residual factors for significantly intense reflections: 0.1264
• Weighted residual factors for all reflections included in the refinement: 0.1377
• Goodness-of-fit parameter for all reflections included in the refinement: 1.033
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No