Information card for entry 4073775

Structure parameters

• Formula: C32.5 H46 Ge N2
• Calculated formula: C32.5 H46 Ge N2
• Title of publication: Stabilization of a Transient Diorganogermylene by an N-Heterocyclic Carbene
• Authors of publication: Rupar, Paul A.; Jennings, Michael C.; Ragogna, Paul J.; Baines, Kim M.
• Journal of publication: Organometallics
• Year of publication: 2007
• Journal volume: 26
• Journal issue: 17
• Pages of publication: 4109
• a: 8.8091 ± 0.0009 Å
• b: 13.7282 ± 0.0017 Å
• c: 14.061 ± 0.002 Å
• α: 63.736 ± 0.005°
• β: 80.017 ± 0.007°
• γ: 81.165 ± 0.008°
• Cell volume: 1496.1 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0678
• Residual factor for significantly intense reflections: 0.0509
• Weighted residual factors for significantly intense reflections: 0.1246
• Weighted residual factors for all reflections included in the refinement: 0.1347
• Goodness-of-fit parameter for all reflections included in the refinement: 1.022
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No