Information card for entry 4073776

Structure parameters

• Formula: C32 H48 B Ge N2
• Calculated formula: C32 H48 B Ge N2
• Title of publication: Stabilization of a Transient Diorganogermylene by an N-Heterocyclic Carbene
• Authors of publication: Rupar, Paul A.; Jennings, Michael C.; Ragogna, Paul J.; Baines, Kim M.
• Journal of publication: Organometallics
• Year of publication: 2007
• Journal volume: 26
• Journal issue: 17
• Pages of publication: 4109
• a: 22.0634 ± 0.0005 Å
• b: 8.6076 ± 0.0002 Å
• c: 16.2745 ± 0.0005 Å
• α: 90°
• β: 93.096 ± 0.001°
• γ: 90°
• Cell volume: 3086.23 ± 0.14 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0524
• Residual factor for significantly intense reflections: 0.0365
• Weighted residual factors for significantly intense reflections: 0.087
• Weighted residual factors for all reflections included in the refinement: 0.0924
• Goodness-of-fit parameter for all reflections included in the refinement: 1.078
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No