Crystallography Open Database

Information card for entry 4073777

Preview

Coordinates	4073777.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C38 H49 N2 Rh
Calculated formula	C38 H49 N2 Rh
Title of publication	Alkyl and Aryl Compounds of Rhodium(III) and Iridium(III) Supported by 4,4‘-Di-tert-butyl-2,2‘-bipyridyl
Authors of publication	Sau, Yiu-Keung; Chan, Ka-Wang; Zhang, Qian-Feng; Williams, Ian D.; Leung, Wa-Hung
Journal of publication	Organometallics
Year of publication	2007
Journal volume	26
Journal issue	25
Pages of publication	6338
a	11.2443 ± 0.0008 Å
b	11.9747 ± 0.0009 Å
c	13.7764 ± 0.001 Å
α	106.461 ± 0.001°
β	102.615 ± 0.001°
γ	102.157 ± 0.001°
Cell volume	1660.8 ± 0.2 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0663
Residual factor for significantly intense reflections	0.0452
Weighted residual factors for significantly intense reflections	0.0813
Weighted residual factors for all reflections included in the refinement	0.0865
Goodness-of-fit parameter for all reflections included in the refinement	1.005
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4073777.html