Information card for entry 4073858

Structure parameters

• Formula: C76 H87 Au4 B20 Cl4 P4 Sn2
• Calculated formula: C76 H87 Au4 B20 Cl4 P4 Sn2
• Title of publication: 1,2-Carbastanna-closo-dodecaborate, a New Tin Ligand in Coordination Chemistry: Synthesis, Structure, and Reactivity
• Authors of publication: Joosten, Dominik; Weissinger, Ines; Kirchmann, Marius; Maichle-Mössmer, Cäcilia; Schappacher, Falko M.; Pöttgen, Rainer; Wesemann, Lars
• Journal of publication: Organometallics
• Year of publication: 2007
• Journal volume: 26
• Journal issue: 23
• Pages of publication: 5696
• a: 25.1882 ± 0.0017 Å
• b: 20.2044 ± 0.0009 Å
• c: 35.831 ± 0.002 Å
• α: 90°
• β: 101.118 ± 0.005°
• γ: 90°
• Cell volume: 17892.6 ± 1.8 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1663
• Residual factor for significantly intense reflections: 0.0788
• Weighted residual factors for significantly intense reflections: 0.1068
• Weighted residual factors for all reflections included in the refinement: 0.1256
• Goodness-of-fit parameter for all reflections included in the refinement: 1.017
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No