Information card for entry 4073859

Structure parameters

• Formula: C72 H137 B30 Cl2 N2 P2 Rh Sn3
• Calculated formula: C72 H137 B30 Cl2 N2 P2 Rh Sn3
• Title of publication: 1,2-Carbastanna-closo-dodecaborate, a New Tin Ligand in Coordination Chemistry: Synthesis, Structure, and Reactivity
• Authors of publication: Joosten, Dominik; Weissinger, Ines; Kirchmann, Marius; Maichle-Mössmer, Cäcilia; Schappacher, Falko M.; Pöttgen, Rainer; Wesemann, Lars
• Journal of publication: Organometallics
• Year of publication: 2007
• Journal volume: 26
• Journal issue: 23
• Pages of publication: 5696
• a: 17.6722 ± 0.0008 Å
• b: 22.529 ± 0.0007 Å
• c: 24.2283 ± 0.001 Å
• α: 90°
• β: 99.158 ± 0.003°
• γ: 90°
• Cell volume: 9523.2 ± 0.7 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0895
• Residual factor for significantly intense reflections: 0.0572
• Weighted residual factors for significantly intense reflections: 0.0971
• Weighted residual factors for all reflections included in the refinement: 0.1075
• Goodness-of-fit parameter for all reflections included in the refinement: 1.079
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No