Crystallography Open Database

Information card for entry 4073932

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Coordinates	4073932.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C37 H44 N2 O8 Rh
Calculated formula	C37 H44 N2 O8 Rh
Title of publication	Cross-Coupling of Alkynes Catalyzed by Phebox−Rhodium Acetate Complexes
Authors of publication	Ito, Jun-ichi; Kitase, Megumi; Nishiyama, Hisao
Journal of publication	Organometallics
Year of publication	2007
Journal volume	26
Journal issue	25
Pages of publication	6412
a	9.437 ± 0.01 Å
b	9.469 ± 0.011 Å
c	19.68 ± 0.02 Å
α	89.08 ± 0.02°
β	84.11 ± 0.03°
γ	86.76 ± 0.02°
Cell volume	1746 ± 3 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1103
Residual factor for significantly intense reflections	0.085
Weighted residual factors for significantly intense reflections	0.1923
Weighted residual factors for all reflections included in the refinement	0.2045
Goodness-of-fit parameter for all reflections included in the refinement	1.11
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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