Crystallography Open Database

Information card for entry 4073933

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Coordinates	4073933.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C203 H224 Cl8 O12 P8 Pd4
Calculated formula	C203 H224 Cl8 O12 P8 Pd4
Title of publication	Asymmetric Hydroformylation of Olefins with Rh Catalysts Modified with Chiral Phosphine−Phosphite Ligands
Authors of publication	Rubio, Miguel; Suárez, Andrés; Álvarez, Eleuterio; Bianchini, Claudio; Oberhauser, Werner; Peruzzini, Maurizio; Pizzano, Antonio
Journal of publication	Organometallics
Year of publication	2007
Journal volume	26
Journal issue	25
Pages of publication	6428
a	21.3901 ± 0.0011 Å
b	10.2591 ± 0.0004 Å
c	23.6159 ± 0.0012 Å
α	90°
β	111.582 ± 0.001°
γ	90°
Cell volume	4819 ± 0.4 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	6
Space group number	4
Hermann-Mauguin space group symbol	P 1 21 1
Hall space group symbol	P 2yb
Residual factor for all reflections	0.1042
Residual factor for significantly intense reflections	0.0646
Weighted residual factors for significantly intense reflections	0.1575
Weighted residual factors for all reflections included in the refinement	0.1823
Goodness-of-fit parameter for all reflections included in the refinement	1.037
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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