Information card for entry 4074778

Structure parameters

• Formula: C73 H80 I2 O4 P4 S4 Tm2
• Calculated formula: C66 H72 I2 O4 P4 S4 Tm2
• Title of publication: Thulium Alkylidene Complexes: Synthesis, X-ray Structures, and Reactivity
• Authors of publication: Cantat, Thibault; Jaroschik, Florian; Ricard, Louis; Le Floch, Pascal; Nief, François; Mézailles, Nicolas
• Journal of publication: Organometallics
• Year of publication: 2006
• Journal volume: 25
• Journal issue: 5
• Pages of publication: 1329 - 1332
• a: 19.756 ± 0.001 Å
• b: 20.68 ± 0.001 Å
• c: 18.302 ± 0.001 Å
• α: 90°
• β: 95.87 ± 0.001°
• γ: 90°
• Cell volume: 7438.1 ± 0.7 ų
• Cell temperature: 150 ± 0.1 K
• Ambient diffraction temperature: 150 ± 0.1 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.07
• Residual factor for significantly intense reflections: 0.0469
• Weighted residual factors for significantly intense reflections: 0.1257
• Weighted residual factors for all reflections included in the refinement: 0.1347
• Goodness-of-fit parameter for all reflections included in the refinement: 1.004
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No