Crystallography Open Database

Information card for entry 4075497

Preview

Coordinates	4075497.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C39 H31 O3 Os Sn2
Calculated formula	C39 H31 O3 Os Sn2
Title of publication	Cluster Fragmentation and Facile Cleavage of Phenyl Groups from the SnPh3Ligand in Reactions of Os3(CO)11(SnPh3)(μ-H) with CO and HSnPh3
Authors of publication	Adams, Richard D.; Captain, Burjor; Zhu, Lei
Journal of publication	Organometallics
Year of publication	2006
Journal volume	25
Journal issue	17
Pages of publication	4183
a	11.224 ± 0.0003 Å
b	11.3303 ± 0.0003 Å
c	16.097 ± 0.0004 Å
α	93.721 ± 0.001°
β	109.943 ± 0.001°
γ	110.146 ± 0.001°
Cell volume	1767.59 ± 0.08 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0232
Residual factor for significantly intense reflections	0.0198
Weighted residual factors for significantly intense reflections	0.0496
Weighted residual factors for all reflections included in the refinement	0.0572
Goodness-of-fit parameter for all reflections included in the refinement	1.149
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4075497.html