Information card for entry 4075498

Structure parameters

• Formula: C22 H16 O4 Os Sn
• Calculated formula: C22 H16 O4 Os Sn
• SMILES: [OsH]([Sn](c1ccccc1)(c1ccccc1)c1ccccc1)(C#[O])(C#[O])(C#[O])C#[O]
• Title of publication: Cluster Fragmentation and Facile Cleavage of Phenyl Groups from the SnPh3Ligand in Reactions of Os3(CO)11(SnPh3)(μ-H) with CO and HSnPh3
• Authors of publication: Adams, Richard D.; Captain, Burjor; Zhu, Lei
• Journal of publication: Organometallics
• Year of publication: 2006
• Journal volume: 25
• Journal issue: 17
• Pages of publication: 4183
• a: 9.667 ± 0.0004 Å
• b: 10.8704 ± 0.0004 Å
• c: 11.2785 ± 0.0004 Å
• α: 67.827 ± 0.001°
• β: 88.862 ± 0.001°
• γ: 83.898 ± 0.001°
• Cell volume: 1091.06 ± 0.07 ų
• Cell temperature: 294 ± 2 K
• Ambient diffraction temperature: 294 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0224
• Residual factor for significantly intense reflections: 0.0195
• Weighted residual factors for significantly intense reflections: 0.0469
• Weighted residual factors for all reflections included in the refinement: 0.0483
• Goodness-of-fit parameter for all reflections included in the refinement: 1.051
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No