Crystallography Open Database

Information card for entry 4075693

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Coordinates	4075693.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H42 Cl3 O P2 Rh
Calculated formula	C32 H42 Cl3 O P2 Rh
Title of publication	Nine-Membered Trans Square-Planar Chelates Formed by a bisbi Analogue
Authors of publication	Eberhard, Michael R.; Heslop, Katie M.; Orpen, A. Guy; Pringle, Paul G.
Journal of publication	Organometallics
Year of publication	2005
Journal volume	24
Journal issue	3
Pages of publication	335
a	16.7591 ± 0.0014 Å
b	11.2544 ± 0.0009 Å
c	17.1493 ± 0.0015 Å
α	90°
β	102.501 ± 0.002°
γ	90°
Cell volume	3157.9 ± 0.5 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	9
Hermann-Mauguin space group symbol	C 1 c 1
Hall space group symbol	C -2yc
Residual factor for all reflections	0.0329
Residual factor for significantly intense reflections	0.0286
Weighted residual factors for significantly intense reflections	0.0615
Weighted residual factors for all reflections included in the refinement	0.063
Goodness-of-fit parameter for all reflections included in the refinement	1.013
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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