Information card for entry 4075789

Structure parameters

• Formula: C49 H40 Cl4 I N2 O3 P2 Rh
• Calculated formula: C49 H40 Cl4 I N2 O3 P2 Rh
• Title of publication: Rhodium-Catalyzed Dimerization of Terminal Alkynes Assisted by MeI
• Authors of publication: Lee, Chrong-Ching; Lin, Ying-Chih; Liu, Yi-Hung; Wang, Yu
• Journal of publication: Organometallics
• Year of publication: 2005
• Journal volume: 24
• Journal issue: 1
• Pages of publication: 136
• a: 12.915 ± 0.002 Å
• b: 13.21 ± 0.003 Å
• c: 15.975 ± 0.003 Å
• α: 77.06 ± 0.02°
• β: 71.678 ± 0.013°
• γ: 66.884 ± 0.015°
• Cell volume: 2363.7 ± 0.8 ų
• Cell temperature: 295 ± 2 K
• Ambient diffraction temperature: 295 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0738
• Residual factor for significantly intense reflections: 0.0454
• Weighted residual factors for all reflections: 0.1475
• Weighted residual factors for significantly intense reflections: 0.1301
• Goodness-of-fit parameter for all reflections: 0.943
• Goodness-of-fit parameter for significantly intense reflections: 1.007
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No