Information card for entry 4075833

Structure parameters

• Formula: C24 H33 N2 P Pb Si2
• Calculated formula: C24 H33 N2 P Pb Si2
• SMILES: C1=c2ccccn2[Pb](N([Si](C)(C)C)[Si](C)(C)C)[P]1(c1ccccc1)c1ccccc1
• Title of publication: A Heterotopically Chelated Low-Valent Lead Amide1
• Authors of publication: Murso, Alexander; Straka, Michal; Kaupp, Martin; Bertermann, Rüdiger; Stalke, Dietmar
• Journal of publication: Organometallics
• Year of publication: 2005
• Journal volume: 24
• Journal issue: 14
• Pages of publication: 3576
• a: 8.5944 ± 0.0015 Å
• b: 17.482 ± 0.003 Å
• c: 18.411 ± 0.003 Å
• α: 102.425 ± 0.003°
• β: 96.536 ± 0.003°
• γ: 95.131 ± 0.003°
• Cell volume: 2665.3 ± 0.8 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0206
• Residual factor for significantly intense reflections: 0.0179
• Weighted residual factors for significantly intense reflections: 0.0405
• Weighted residual factors for all reflections included in the refinement: 0.0412
• Goodness-of-fit parameter for all reflections included in the refinement: 1.085
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No