Resolution and Improved Synthesis of (±)-Arsenicin A: A Natural Adamantane-Type Tetraarsenical Possessing Strong Anti-Acute Promelocytic Leukemia Cell Line Activity
Authors of publication
Lu, Di; Coote, Michelle L.; Ho, Junming; Kilah, Nathan L.; Lin, Ching-Yeh; Salem, Geoff; Weir, Michelle L.; Willis, Anthony C.; Wild, S. Bruce; Dilda, Pierre J.
Journal of publication
Organometallics
Year of publication
2012
Journal volume
31
Journal issue
5
Pages of publication
1808
a
9.3774 ± 0.0002 Å
b
19.0852 ± 0.0003 Å
c
10.0191 ± 0.0002 Å
α
90°
β
94.8205 ± 0.0013°
γ
90°
Cell volume
1786.77 ± 0.06 Å3
Cell temperature
200 K
Ambient diffraction temperature
200 K
Number of distinct elements
4
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/c 1
Hall space group symbol
-P 2ybc
Residual factor for all reflections
0.0376
Residual factor for significantly intense reflections
0.0318
Weighted residual factors for all reflections
0.0831
Weighted residual factors for significantly intense reflections
0.078
Weighted residual factors for all reflections included in the refinement
0.0831
Goodness-of-fit parameter for all reflections included in the refinement
