Resolution and Improved Synthesis of (±)-Arsenicin A: A Natural Adamantane-Type Tetraarsenical Possessing Strong Anti-Acute Promelocytic Leukemia Cell Line Activity
Authors of publication
Lu, Di; Coote, Michelle L.; Ho, Junming; Kilah, Nathan L.; Lin, Ching-Yeh; Salem, Geoff; Weir, Michelle L.; Willis, Anthony C.; Wild, S. Bruce; Dilda, Pierre J.
Journal of publication
Organometallics
Year of publication
2012
Journal volume
31
Journal issue
5
Pages of publication
1808
a
6.8594 ± 0.0003 Å
b
9.8038 ± 0.0005 Å
c
12.3203 ± 0.0006 Å
α
90°
β
90°
γ
90°
Cell volume
828.52 ± 0.07 Å3
Cell temperature
150 K
Ambient diffraction temperature
150 K
Number of distinct elements
4
Space group number
19
Hermann-Mauguin space group symbol
P 21 21 21
Hall space group symbol
P 2ac 2ab
Residual factor for all reflections
0.0414
Residual factor for significantly intense reflections
0.0355
Weighted residual factors for all reflections
0.0835
Weighted residual factors for significantly intense reflections
0.0804
Weighted residual factors for all reflections included in the refinement
0.0835
Goodness-of-fit parameter for all reflections included in the refinement
