Information card for entry 4076544

Structure parameters

• Formula: C18 H42 Cl Ge N2 P Si
• Calculated formula: C18 H42 Cl Ge N2 P Si
• SMILES: [Ge]1(P(C(C)(C)C)C(C)(C)C)(Cl)N([Si](N1C(C)(C)C)(C)C)C(C)(C)C
• Title of publication: Insertions of Cyclic and Acyclic Germanium and Tin Heterocarbenoids into Phosphorus‒Chlorine Bonds: Syntheses, Structures, and Reactivities
• Authors of publication: West, Joseph K.; Stahl, Lothar
• Journal of publication: Organometallics
• Year of publication: 2012
• Journal volume: 31
• Journal issue: 5
• Pages of publication: 2042
• a: 11.2153 ± 0.0012 Å
• b: 11.8227 ± 0.0013 Å
• c: 18.439 ± 0.002 Å
• α: 90°
• β: 93.948 ± 0.002°
• γ: 90°
• Cell volume: 2439.1 ± 0.5 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0288
• Residual factor for significantly intense reflections: 0.0256
• Weighted residual factors for significantly intense reflections: 0.0721
• Weighted residual factors for all reflections included in the refinement: 0.0742
• Goodness-of-fit parameter for all reflections included in the refinement: 1.055
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No