Information card for entry 4076545

Structure parameters

• Formula: C41 H98 Cl4 Ge4 N8 P2 Si4
• Calculated formula: C41 H98 Cl4 Ge4 N8 P2 Si4
• Title of publication: Insertions of Cyclic and Acyclic Germanium and Tin Heterocarbenoids into Phosphorus‒Chlorine Bonds: Syntheses, Structures, and Reactivities
• Authors of publication: West, Joseph K.; Stahl, Lothar
• Journal of publication: Organometallics
• Year of publication: 2012
• Journal volume: 31
• Journal issue: 5
• Pages of publication: 2042
• a: 17.6548 ± 0.0007 Å
• b: 17.6548 ± 0.0007 Å
• c: 10.5683 ± 0.0008 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3294.1 ± 0.3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 81
• Hermann-Mauguin space group symbol: P -4
• Hall space group symbol: P -4
• Residual factor for all reflections: 0.0232
• Residual factor for significantly intense reflections: 0.0218
• Weighted residual factors for significantly intense reflections: 0.0593
• Weighted residual factors for all reflections included in the refinement: 0.06
• Goodness-of-fit parameter for all reflections included in the refinement: 1.039
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No