Information card for entry 4076589

Structure parameters

• Formula: C28.5 H20 B F15 Si
• Calculated formula: C28.5 H20 B F15 Si
• Title of publication: Preparation of Dihydroborole Derivatives by a Simple 1,1-Carboboration Route
• Authors of publication: Feldmann, Andreas; Iida, Azusa; Fröhlich, Roland; Yamaguchi, Shigehiro; Kehr, Gerald; Erker, Gerhard
• Journal of publication: Organometallics
• Year of publication: 2012
• Journal volume: 31
• Journal issue: 6
• Pages of publication: 2445
• a: 7.4428 ± 0.0002 Å
• b: 12.5739 ± 0.001 Å
• c: 16.1379 ± 0.0005 Å
• α: 92.161 ± 0.003°
• β: 102.917 ± 0.002°
• γ: 100.476 ± 0.004°
• Cell volume: 1442.67 ± 0.13 ų
• Cell temperature: 223 ± 2 K
• Ambient diffraction temperature: 223 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0419
• Residual factor for significantly intense reflections: 0.0409
• Weighted residual factors for significantly intense reflections: 0.1133
• Weighted residual factors for all reflections included in the refinement: 0.1144
• Goodness-of-fit parameter for all reflections included in the refinement: 1.054
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No