Information card for entry 4076590

Structure parameters

• Common name: Ni2Lig2
• Formula: C19.5 H26.25 N1.5 Ni0.75 O0.75
• Calculated formula: C19.5 H21 N3 Ni0.75 O0.75
• Title of publication: Difference in the Reactivities of H- and Me-Substituted Dinucleating Bis(iminopyridine) Ligands with Nickel(0)
• Authors of publication: Bheemaraju, Amarnath; Lord, Richard L.; Müller, Peter; Groysman, Stanislav
• Journal of publication: Organometallics
• Year of publication: 2012
• Journal volume: 31
• Journal issue: 6
• Pages of publication: 2120
• a: 13.7434 ± 0.0011 Å
• b: 16.1755 ± 0.0013 Å
• c: 16.5521 ± 0.0014 Å
• α: 91.446 ± 0.001°
• β: 97.41 ± 0.001°
• γ: 103.874 ± 0.001°
• Cell volume: 3536.4 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0646
• Residual factor for significantly intense reflections: 0.048
• Weighted residual factors for significantly intense reflections: 0.1221
• Weighted residual factors for all reflections included in the refinement: 0.1334
• Goodness-of-fit parameter for all reflections included in the refinement: 1.034
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No