Information card for entry 4076708

Structure parameters

• Formula: C148.75 H109.5 Cl1.5 O16 Os6 P6 Sb2
• Calculated formula: C148.75 H109.5 Cl1.5 O16 Os6 P6 Sb2
• Title of publication: Nucleophilic Addition Reactions of the Osmium−Antimony Cluster (μ-H)Os3(CO)9(μ3-C6H4)(μ-SbPh2): Orthometalation of Triphenylphosphine at Ambient Temperature
• Authors of publication: Chen, Guizhu; Deng, Mingli; Lee, Chee Keong; Leong, Weng Kee
• Journal of publication: Organometallics
• Year of publication: 2002
• Journal volume: 21
• Journal issue: 6
• Pages of publication: 1227
• a: 13.4047 ± 0.0001 Å
• b: 23.8087 ± 0.0003 Å
• c: 26.2516 ± 0.0001 Å
• α: 64.522 ± 0.001°
• β: 82.59 ± 0.001°
• γ: 89.91 ± 0.001°
• Cell volume: 7486.61 ± 0.13 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1335
• Residual factor for significantly intense reflections: 0.0715
• Weighted residual factors for significantly intense reflections: 0.1657
• Weighted residual factors for all reflections included in the refinement: 0.1996
• Goodness-of-fit parameter for all reflections included in the refinement: 1.039
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No