Information card for entry 4076783

Structure parameters

• Formula: C18 H32 O2 Si2 W
• Calculated formula: C18 H32 O2 Si2 W
• Title of publication: Synthesis of Self-Stabilized and Donor-Free Silyl(silylene)tungsten Complexes
• Authors of publication: Ueno, Keiji; Asami, Satsuki; Watanabe, Nobuhiko; Ogino, Hiroshi
• Journal of publication: Organometallics
• Year of publication: 2002
• Journal volume: 21
• Journal issue: 7
• Pages of publication: 1326
• a: 9.184 ± 0.003 Å
• b: 26.208 ± 0.009 Å
• c: 9.354 ± 0.003 Å
• α: 90°
• β: 112.43 ± 0.02°
• γ: 90°
• Cell volume: 2081.1 ± 1.2 ų
• Cell temperature: 150 ± 1 K
• Ambient diffraction temperature: 150 ± 1 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/a 1
• Hall space group symbol: -P 2yab
• Residual factor for all reflections: 0.0756
• Residual factor for significantly intense reflections: 0.0578
• Weighted residual factors for significantly intense reflections: 0.1524
• Weighted residual factors for all reflections included in the refinement: 0.1669
• Goodness-of-fit parameter for all reflections included in the refinement: 1.029
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No