Information card for entry 4076877

Structure parameters

• Formula: C19 H11 N O9 Os3 S
• Calculated formula: C19 H11 N O9 Os3 S
• SMILES: [Os]12([Os]3([Os]1([n]1c4c3cccc4sc1C)(C#[O])(C#[O])(C2)C)(C#[O])(C#[O])C#[O])(C#[O])(C#[O])(C#[O])C#[O]
• Title of publication: Reaction of Os3(CO)9(μ3-η2-C7H3(2-CH3)NS)(μ-H) with Diazomethane. The First Example of a Trimetallic Cluster Containing a μ-Methylidene and a σ-Methyl
• Authors of publication: Kabir, Shariff E.; Malik, K. M. Abdul; Mandal, Himadri S.; Mottalib, Md. Abdul; Abedin, Md. Joynal; Rosenberg, Edward
• Journal of publication: Organometallics
• Year of publication: 2002
• Journal volume: 21
• Journal issue: 13
• Pages of publication: 2593
• a: 9.2852 ± 0.0004 Å
• b: 10.3219 ± 0.0004 Å
• c: 13.4911 ± 0.0005 Å
• α: 97.974 ± 0.003°
• β: 105.797 ± 0.003°
• γ: 112.489 ± 0.002°
• Cell volume: 1105.83 ± 0.08 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0536
• Residual factor for significantly intense reflections: 0.0412
• Weighted residual factors for all reflections: 0.0991
• Weighted residual factors for significantly intense reflections: 0.0931
• Goodness-of-fit parameter for all reflections: 1.017
• Goodness-of-fit parameter for significantly intense reflections: 1.056
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No