Information card for entry 4076878

Structure parameters

• Formula: C17 H9 N O8 Os3 S
• Calculated formula: C17 H9 N O8 Os3 S
• SMILES: [Os]1234([Os]56([Os]71([n]1c8c(C257)cccc8sc1C)(C#[O])(C#[O])([H]4)[H]6)(C#[O])(C#[O])(C#[O])[H]3)(C#[O])(C#[O])C#[O]
• Title of publication: Reaction of Os3(CO)9(μ3-η2-C7H3(2-CH3)NS)(μ-H) with Diazomethane. The First Example of a Trimetallic Cluster Containing a μ-Methylidene and a σ-Methyl
• Authors of publication: Kabir, Shariff E.; Malik, K. M. Abdul; Mandal, Himadri S.; Mottalib, Md. Abdul; Abedin, Md. Joynal; Rosenberg, Edward
• Journal of publication: Organometallics
• Year of publication: 2002
• Journal volume: 21
• Journal issue: 13
• Pages of publication: 2593
• a: 16.1881 ± 0.0004 Å
• b: 11.2807 ± 0.0004 Å
• c: 11.8325 ± 0.0004 Å
• α: 90°
• β: 100.692 ± 0.0018°
• γ: 90°
• Cell volume: 2123.26 ± 0.12 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0729
• Residual factor for significantly intense reflections: 0.0459
• Weighted residual factors for all reflections: 0.1083
• Weighted residual factors for significantly intense reflections: 0.098
• Goodness-of-fit parameter for all reflections: 0.994
• Goodness-of-fit parameter for significantly intense reflections: 1.07
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No