Information card for entry 4076967

Structure parameters

• Formula: C26 H36 O16 P4 Ru4
• Calculated formula: C26 H36 O16 P4 Ru4
• Title of publication: Synthesis, Structures, and Solvent-Occlusion Properties of a Molecular Loop and a Molecular Square Using Tetracarbonyl- and Diphosphine-Ligated Diruthenium(I) as Building Blocks and Dicarboxylates as Linkers
• Authors of publication: Shiu, Kom-Bei; Lee, Hong-Chan; Lee, Gene-Hsiang; Wang, Yu
• Journal of publication: Organometallics
• Year of publication: 2002
• Journal volume: 21
• Journal issue: 19
• Pages of publication: 4013
• a: 9.7864 ± 0.0001 Å
• b: 14.4313 ± 0.0002 Å
• c: 14.6391 ± 0.0002 Å
• α: 87.923 ± 0.0005°
• β: 80.9637 ± 0.0006°
• γ: 87.5714 ± 0.0005°
• Cell volume: 2039.08 ± 0.04 ų
• Cell temperature: 150 ± 1 K
• Ambient diffraction temperature: 150 ± 1 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0548
• Residual factor for significantly intense reflections: 0.0414
• Weighted residual factors for significantly intense reflections: 0.1082
• Weighted residual factors for all reflections included in the refinement: 0.1189
• Goodness-of-fit parameter for all reflections included in the refinement: 1.165
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No