Information card for entry 4076968

Structure parameters

• Formula: C25.5 H39 Cl3 O16 P4 Ru4
• Calculated formula: C25.5 H39 Cl3 O16 P4 Ru4
• Title of publication: Synthesis, Structures, and Solvent-Occlusion Properties of a Molecular Loop and a Molecular Square Using Tetracarbonyl- and Diphosphine-Ligated Diruthenium(I) as Building Blocks and Dicarboxylates as Linkers
• Authors of publication: Shiu, Kom-Bei; Lee, Hong-Chan; Lee, Gene-Hsiang; Wang, Yu
• Journal of publication: Organometallics
• Year of publication: 2002
• Journal volume: 21
• Journal issue: 19
• Pages of publication: 4013
• a: 13.3878 ± 0.0001 Å
• b: 21.4312 ± 0.0002 Å
• c: 15.3354 ± 0.0002 Å
• α: 90°
• β: 95.2705 ± 0.0004°
• γ: 90°
• Cell volume: 4381.38 ± 0.08 ų
• Cell temperature: 150 ± 1 K
• Ambient diffraction temperature: 150 ± 1 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.072
• Residual factor for significantly intense reflections: 0.0457
• Weighted residual factors for significantly intense reflections: 0.1165
• Weighted residual factors for all reflections included in the refinement: 0.1386
• Goodness-of-fit parameter for all reflections included in the refinement: 1.134
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No