Information card for entry 4077367

Structure parameters

• Formula: C27 H39 Br2 Cl3 N4 Pd2
• Calculated formula: C27 H39 Br2 Cl3 N4 Pd2
• Title of publication: Synthesis and Structure of New Binuclear Organopalladium Macrocyclic Complexes
• Authors of publication: Tsubomura, Taro; Tanihata, Takayuki; Yamakawa, Tetsuya; Ohmi, Rakuko; Tamane, Tsuyoshi; Higuchi, Akon; Katoh, Akira; Sakai, Ken
• Journal of publication: Organometallics
• Year of publication: 2001
• Journal volume: 20
• Journal issue: 18
• Pages of publication: 3833
• a: 14.445 ± 0.002 Å
• b: 17.928 ± 0.002 Å
• c: 12.903 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3341.5 ± 0.8 ų
• Cell temperature: 296.2 K
• Number of distinct elements: 6
• Space group number: 62
• Hermann-Mauguin space group symbol: P n m a
• Hall space group symbol: -P 2ac 2n
• Residual factor for significantly intense reflections: 0.0485
• Weighted residual factors for all reflections included in the refinement: 0.1151
• Goodness-of-fit parameter for all reflections included in the refinement: 0.999
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No