Information card for entry 4077368

Structure parameters

• Formula: C11 H19 Cl N Nb O Si
• Calculated formula: C11 H19 Cl N Nb O Si
• Title of publication: Competitive Insertion of Isocyanide and Carbon Dioxide into Niobium− and Silicon−Amido Bonds
• Authors of publication: Alcalde, M. Isabel; Gómez-Sal, M. Pilar; Royo, Pascual
• Journal of publication: Organometallics
• Year of publication: 2001
• Journal volume: 20
• Journal issue: 22
• Pages of publication: 4623
• a: 7.437 ± 0.001 Å
• b: 8.818 ± 0.001 Å
• c: 11.819 ± 0.001 Å
• α: 78.24 ± 0.01°
• β: 80.97 ± 0.01°
• γ: 81.65 ± 0.01°
• Cell volume: 744.25 ± 0.15 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.024
• Residual factor for significantly intense reflections: 0.0219
• Weighted residual factors for significantly intense reflections: 0.0591
• Weighted residual factors for all reflections included in the refinement: 0.0604
• Goodness-of-fit parameter for all reflections included in the refinement: 1.011
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No