Information card for entry 4077615

Structure parameters

• Formula: C21 H59.25 Cu P3 Se Si
• Calculated formula: C21 H59.25 Cu P3 Se Si
• Title of publication: Synthesis and Characterization of Tris(trialkylphosphine)copper(I)trimethylsilylchalcogenolates
• Authors of publication: Tran, Diem T. T.; Corrigan, John F.
• Journal of publication: Organometallics
• Year of publication: 2000
• Journal volume: 19
• Journal issue: 24
• Pages of publication: 5202
• a: 16.7522 ± 0.0007 Å
• b: 11.6163 ± 0.0003 Å
• c: 17.4349 ± 0.0007 Å
• α: 90°
• β: 117.278 ± 0.0014°
• γ: 90°
• Cell volume: 3015.5 ± 0.2 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0921
• Residual factor for significantly intense reflections: 0.0393
• Weighted residual factors for significantly intense reflections: 0.0786
• Weighted residual factors for all reflections included in the refinement: 0.0886
• Goodness-of-fit parameter for all reflections included in the refinement: 0.943
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No