Information card for entry 4077699

Structure parameters

• Formula: C36 H49 F3 Si
• Calculated formula: C36 H49 F3.003 Si
• Title of publication: Reduction of Terphenyltrifluorosilanes: C−C Insertion Products and Possible Formation of a Disilyne
• Authors of publication: Pietschnig, Rudolf; West, Robert; Powell, Douglas R.
• Journal of publication: Organometallics
• Year of publication: 2000
• Journal volume: 19
• Journal issue: 14
• Pages of publication: 2724
• a: 10.9496 ± 0.0004 Å
• b: 12.0899 ± 0.0005 Å
• c: 25.4843 ± 0.0009 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3373.6 ± 0.2 ų
• Cell temperature: 133 ± 2 K
• Ambient diffraction temperature: 133 ± 2 K
• Number of distinct elements: 4
• Space group number: 57
• Hermann-Mauguin space group symbol: P b c m
• Hall space group symbol: -P 2c 2b
• Residual factor for all reflections: 0.0672
• Residual factor for significantly intense reflections: 0.0569
• Weighted residual factors for significantly intense reflections: 0.1433
• Weighted residual factors for all reflections included in the refinement: 0.1481
• Goodness-of-fit parameter for all reflections included in the refinement: 1.106
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No