Information card for entry 4078993

Structure parameters

• Formula: C32 H52 F N9 O12 Si8
• Calculated formula: C32 H52 F N9 O12 Si8
• Title of publication: Facile Synthesis of Novel Functionalized Silsesquioxane Nanostructures Containing an Encapsulated Fluoride Anion
• Authors of publication: El Aziz, Youssef; Bassindale, Alan R.; Taylor, Peter G.; Horton, Peter N.; Stephenson, Richard A.; Hursthouse, Michael B.
• Journal of publication: Organometallics
• Year of publication: 2012
• Journal volume: 31
• Journal issue: 17
• Pages of publication: 6032
• a: 8.6557 ± 0.0002 Å
• b: 11.7528 ± 0.0002 Å
• c: 12.4208 ± 0.0002 Å
• α: 106.041 ± 0.001°
• β: 98.006 ± 0.001°
• γ: 96.123 ± 0.001°
• Cell volume: 1188.45 ± 0.04 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0388
• Residual factor for significantly intense reflections: 0.0342
• Weighted residual factors for significantly intense reflections: 0.1053
• Weighted residual factors for all reflections included in the refinement: 0.1083
• Goodness-of-fit parameter for all reflections included in the refinement: 1.16
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No