Information card for entry 4080715

Structure parameters

• Formula: C24 H39 Lu Si3
• Calculated formula: C24 H39 Lu Si3
• SMILES: [Lu]123456789%10%11%12([cH]%13[cH]1[cH]2[cH]3[c]4%13[Si](C)(C)C)([cH]1[cH]5[cH]6[cH]7[c]81[Si](C)(C)C)[cH]1[cH]9[cH]%10[cH]%11[c]%121[Si](C)(C)C
• Title of publication: Synthetic Aspects of (C5H4SiMe3)3Ln Rare-Earth Chemistry: Formation of (C5H4SiMe3)3Lu via [(C5H4SiMe3)2Ln]+Metallocene Precursors
• Authors of publication: Peterson, Jeffrey K.; MacDonald, Matthew R.; Ziller, Joseph W.; Evans, William J.
• Journal of publication: Organometallics
• Year of publication: 2013
• Journal volume: 32
• Journal issue: 9
• Pages of publication: 2625
• a: 8.1546 ± 0.0004 Å
• b: 22.3062 ± 0.0011 Å
• c: 28.6176 ± 0.0014 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 5205.5 ± 0.4 ų
• Cell temperature: 83 ± 2 K
• Ambient diffraction temperature: 83 ± 2 K
• Number of distinct elements: 4
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0218
• Residual factor for significantly intense reflections: 0.0181
• Weighted residual factors for significantly intense reflections: 0.0397
• Weighted residual factors for all reflections included in the refinement: 0.0412
• Goodness-of-fit parameter for all reflections included in the refinement: 1.108
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No