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Information card for entry 4080716
Preview
Coordinates | 4080716.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C82 H130 Lu4 Si8 |
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Calculated formula | C82 H130 Lu4 Si8 |
Title of publication | Synthetic Aspects of (C5H4SiMe3)3Ln Rare-Earth Chemistry: Formation of (C5H4SiMe3)3Lu via [(C5H4SiMe3)2Ln]+Metallocene Precursors |
Authors of publication | Peterson, Jeffrey K.; MacDonald, Matthew R.; Ziller, Joseph W.; Evans, William J. |
Journal of publication | Organometallics |
Year of publication | 2013 |
Journal volume | 32 |
Journal issue | 9 |
Pages of publication | 2625 |
a | 10.7315 ± 0.0006 Å |
b | 12.7032 ± 0.0007 Å |
c | 17.8457 ± 0.001 Å |
α | 101.1 ± 0.0006° |
β | 99.6938 ± 0.0006° |
γ | 107.192 ± 0.0005° |
Cell volume | 2213.8 ± 0.2 Å3 |
Cell temperature | 143 ± 2 K |
Ambient diffraction temperature | 143 ± 2 K |
Number of distinct elements | 4 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0226 |
Residual factor for significantly intense reflections | 0.0201 |
Weighted residual factors for significantly intense reflections | 0.0489 |
Weighted residual factors for all reflections included in the refinement | 0.05 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.022 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4080716.html
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Users of the data should acknowledge the original authors of the
structural data.