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Information card for entry 4080717
Preview
Coordinates | 4080717.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C52 H70 B Lu O3 Si2 |
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Calculated formula | C52 H70 B Lu O3 Si2 |
Title of publication | Synthetic Aspects of (C5H4SiMe3)3Ln Rare-Earth Chemistry: Formation of (C5H4SiMe3)3Lu via [(C5H4SiMe3)2Ln]+Metallocene Precursors |
Authors of publication | Peterson, Jeffrey K.; MacDonald, Matthew R.; Ziller, Joseph W.; Evans, William J. |
Journal of publication | Organometallics |
Year of publication | 2013 |
Journal volume | 32 |
Journal issue | 9 |
Pages of publication | 2625 |
a | 13.8245 ± 0.0008 Å |
b | 19.0919 ± 0.0012 Å |
c | 19.5594 ± 0.0012 Å |
α | 87.268 ± 0.0007° |
β | 76.6168 ± 0.0007° |
γ | 78.7567 ± 0.0007° |
Cell volume | 4925.8 ± 0.5 Å3 |
Cell temperature | 143 ± 2 K |
Ambient diffraction temperature | 143 ± 2 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0594 |
Residual factor for significantly intense reflections | 0.0477 |
Weighted residual factors for significantly intense reflections | 0.1184 |
Weighted residual factors for all reflections included in the refinement | 0.1274 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.032 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4080717.html
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Users of the data should acknowledge the original authors of the
structural data.