Information card for entry 4081042

Structure parameters

• Formula: C49 H50 N2 Ni Sn2
• Calculated formula: C49 H50 N2 Ni Sn2
• Title of publication: Carbon‒Hydrogen Bond Stannylation and Alkylation Catalyzed by Nitrogen-Donor-Supported Nickel Complexes: Intermediates with Ni‒Sn Bonds and Catalytic Carbostannylation of Ethylene with Organostannanes
• Authors of publication: Doster, Meghan E.; Johnson, Samuel A.
• Journal of publication: Organometallics
• Year of publication: 2013
• Journal volume: 32
• Journal issue: 15
• Pages of publication: 4174
• a: 12.288 ± 0.0017 Å
• b: 23.051 ± 0.003 Å
• c: 19.0364 ± 0.0019 Å
• α: 90°
• β: 127.212 ± 0.006°
• γ: 90°
• Cell volume: 4294.3 ± 1 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0505
• Residual factor for significantly intense reflections: 0.0377
• Weighted residual factors for significantly intense reflections: 0.078
• Weighted residual factors for all reflections included in the refinement: 0.0917
• Goodness-of-fit parameter for all reflections included in the refinement: 1.263
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No