Information card for entry 4081043

Structure parameters

• Formula: C49 H51 F5 N4 Ni Sn
• Calculated formula: C49 H51 F5 N4 Ni Sn
• Title of publication: Carbon‒Hydrogen Bond Stannylation and Alkylation Catalyzed by Nitrogen-Donor-Supported Nickel Complexes: Intermediates with Ni‒Sn Bonds and Catalytic Carbostannylation of Ethylene with Organostannanes
• Authors of publication: Doster, Meghan E.; Johnson, Samuel A.
• Journal of publication: Organometallics
• Year of publication: 2013
• Journal volume: 32
• Journal issue: 15
• Pages of publication: 4174
• a: 16.798 ± 0.005 Å
• b: 10.575 ± 0.003 Å
• c: 25.444 ± 0.008 Å
• α: 90°
• β: 90.052 ± 0.004°
• γ: 90°
• Cell volume: 4520 ± 2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 7
• Hermann-Mauguin space group symbol: P 1 c 1
• Hall space group symbol: P -2yc
• Residual factor for all reflections: 0.0777
• Residual factor for significantly intense reflections: 0.0694
• Weighted residual factors for significantly intense reflections: 0.1653
• Weighted residual factors for all reflections included in the refinement: 0.1704
• Goodness-of-fit parameter for all reflections included in the refinement: 1.132
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No