Straightforward Access to Tetrametallic Complexes with a Square Array by Oxidative Dimerization of Organometallic Wires
Authors of publication
Burgun, Alexandre; Gendron, Frédéric; Schauer, Phil A.; Skelton, Brian W.; Low, Paul J.; Costuas, Karine; Halet, Jean-François; Bruce, Michael I.; Lapinte, Claude
Journal of publication
Organometallics
Year of publication
2013
Journal volume
32
Journal issue
18
Pages of publication
5015
a
35.639 ± 0.0018 Å
b
35.639 ± 0.0018 Å
c
9.3223 ± 0.0008 Å
α
90°
β
90°
γ
90°
Cell volume
11840.6 ± 1.3 Å3
Cell temperature
100 ± 2 K
Ambient diffraction temperature
100 ± 2 K
Number of distinct elements
4
Space group number
85
Hermann-Mauguin space group symbol
P 4/n :2
Hall space group symbol
-P 4a
Residual factor for all reflections
0.1514
Residual factor for significantly intense reflections
0.0718
Weighted residual factors for significantly intense reflections
0.16
Weighted residual factors for all reflections included in the refinement
0.1915
Goodness-of-fit parameter for all reflections included in the refinement
