Information card for entry 4081246

Structure parameters

• Formula: C165 H147 As2 Cl4 F12 P8 Ru4
• Calculated formula: C165 H147 As2 Cl4 F12 P8 Ru4
• Title of publication: Straightforward Access to Tetrametallic Complexes with a Square Array by Oxidative Dimerization of Organometallic Wires
• Authors of publication: Burgun, Alexandre; Gendron, Frédéric; Schauer, Phil A.; Skelton, Brian W.; Low, Paul J.; Costuas, Karine; Halet, Jean-François; Bruce, Michael I.; Lapinte, Claude
• Journal of publication: Organometallics
• Year of publication: 2013
• Journal volume: 32
• Journal issue: 18
• Pages of publication: 5015
• a: 17.2467 ± 0.0007 Å
• b: 20.2846 ± 0.0007 Å
• c: 22.0628 ± 0.0009 Å
• α: 98.452 ± 0.003°
• β: 94.541 ± 0.004°
• γ: 95.517 ± 0.003°
• Cell volume: 7565.1 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1067
• Residual factor for significantly intense reflections: 0.0767
• Weighted residual factors for significantly intense reflections: 0.205
• Weighted residual factors for all reflections included in the refinement: 0.2213
• Goodness-of-fit parameter for all reflections included in the refinement: 1.01
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No