Information card for entry 4082805

Structure parameters

• Formula: C40 H65 N7 Si2 Zr
• Calculated formula: C40 H65 N7 Si2 Zr
• Title of publication: Zirconium and Hafnium Hydrazinediido Half-Sandwich Complexes: Synthesis and Reactivity
• Authors of publication: Schweizer, Peter D.; Wadepohl, Hubert; Gade, Lutz H.
• Journal of publication: Organometallics
• Year of publication: 2014
• Journal volume: 33
• Journal issue: 7
• Pages of publication: 1726
• a: 10.97715 ± 0.00014 Å
• b: 18.92432 ± 0.00018 Å
• c: 22.6228 ± 0.0002 Å
• α: 69.7957 ± 0.0009°
• β: 83.7816 ± 0.0009°
• γ: 89.9914 ± 0.0009°
• Cell volume: 4380.93 ± 0.08 ų
• Cell temperature: 110 ± 1 K
• Ambient diffraction temperature: 110 ± 1 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0582
• Residual factor for significantly intense reflections: 0.0501
• Weighted residual factors for significantly intense reflections: 0.134
• Weighted residual factors for all reflections included in the refinement: 0.1415
• Goodness-of-fit parameter for all reflections included in the refinement: 1.073
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.5418 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No