Information card for entry 4082806

Structure parameters

• Formula: C49.5 H66 N6 Si2 Zr
• Calculated formula: C49.5 H66 N6 Si2 Zr
• Title of publication: Zirconium and Hafnium Hydrazinediido Half-Sandwich Complexes: Synthesis and Reactivity
• Authors of publication: Schweizer, Peter D.; Wadepohl, Hubert; Gade, Lutz H.
• Journal of publication: Organometallics
• Year of publication: 2014
• Journal volume: 33
• Journal issue: 7
• Pages of publication: 1726
• a: 11.135 ± 0.007 Å
• b: 11.859 ± 0.007 Å
• c: 19.746 ± 0.01 Å
• α: 79.35 ± 0.008°
• β: 78.097 ± 0.012°
• γ: 68.934 ± 0.014°
• Cell volume: 2363 ± 2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 1 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0779
• Residual factor for significantly intense reflections: 0.0455
• Weighted residual factors for significantly intense reflections: 0.0856
• Weighted residual factors for all reflections included in the refinement: 0.0989
• Goodness-of-fit parameter for all reflections included in the refinement: 1.004
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No