Information card for entry 4083103

Structure parameters

• Formula: C52 H53 F24 N O4 Si2
• Calculated formula: C52 H53 F24 N O4 Si2
• Title of publication: Synthesis and Isolation of a Silylsilicate Containing Two Pentacoordinated Silicon Atoms by Monoprotonation of a Disilicate and Monodeprotonation of a Disilane
• Authors of publication: Kano, Naokazu; Sasaki, Keishi; Miyake, Hideaki; Kawashima, Takayuki
• Journal of publication: Organometallics
• Year of publication: 2014
• Journal volume: 33
• Journal issue: 9
• Pages of publication: 2358
• a: 12.567 ± 0.005 Å
• b: 22.96 ± 0.008 Å
• c: 19.153 ± 0.008 Å
• α: 90°
• β: 99.7765 ± 0.0017°
• γ: 90°
• Cell volume: 5446 ± 4 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1347
• Residual factor for significantly intense reflections: 0.0586
• Weighted residual factors for significantly intense reflections: 0.1092
• Weighted residual factors for all reflections included in the refinement: 0.1391
• Goodness-of-fit parameter for all reflections included in the refinement: 0.929
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No