Information card for entry 4083447

Structure parameters

• Chemical name: [Me3Si4]C4Ru(CO)3
• Formula: C19 H36 O3 Ru Si4
• Calculated formula: C19 H36 O3 Ru Si4
• SMILES: [Ru]123([C]4(=[C]3([Si](C)(C)C)[C]1([Si](C)(C)C)=[C]24[Si](C)(C)C)[Si](C)(C)C)(C#[O])(C#[O])C#[O]
• Title of publication: Tetrasilacyclobutadiene and Cyclobutadiene Tricarbonylruthenium Complexes: [η4-(tBu2MeSi)4Si4]Ru(CO)3and [η4-(Me3Si)4C4]Ru(CO)3
• Authors of publication: Takanashi, Kazunori; Lee, Vladimir Ya.; Sekiguchi, Akira
• Journal of publication: Organometallics
• Year of publication: 2009
• Journal volume: 28
• Journal issue: 4
• Pages of publication: 1248
• a: 9.553 ± 0.0003 Å
• b: 16.194 ± 0.0006 Å
• c: 19.256 ± 0.0005 Å
• α: 90°
• β: 116.648 ± 0.002°
• γ: 90°
• Cell volume: 2662.5 ± 0.15 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 120 ± 1 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0655
• Residual factor for significantly intense reflections: 0.0595
• Weighted residual factors for significantly intense reflections: 0.1711
• Weighted residual factors for all reflections included in the refinement: 0.1746
• Goodness-of-fit parameter for all reflections included in the refinement: 1.158
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No