Information card for entry 4084335

Structure parameters

• Formula: C40 H35 Co F10 N P3
• Calculated formula: C40 H35 Co F10 N P3
• Title of publication: Peripheral Methyl Activation in η4-1,2,3,4-Tetramethylcyclobutadienylcobalt Complexes: Template Synthesis and Subsequent Reactivity of Triphosphamacrocycles
• Authors of publication: Edwards, Peter G.; Kariuki, Benson M.; Newman, Paul D.; Zhang, Wenjian
• Journal of publication: Organometallics
• Year of publication: 2014
• Journal volume: 33
• Journal issue: 19
• Pages of publication: 5440
• a: 15.97 ± 0.0002 Å
• b: 24.4817 ± 0.0003 Å
• c: 19.5063 ± 0.0003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 7626.43 ± 0.18 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 61
• Hermann-Mauguin space group symbol: P c a b
• Hall space group symbol: -P 2bc 2ac
• Residual factor for all reflections: 0.1087
• Residual factor for significantly intense reflections: 0.0463
• Weighted residual factors for significantly intense reflections: 0.0961
• Weighted residual factors for all reflections included in the refinement: 0.1166
• Goodness-of-fit parameter for all reflections included in the refinement: 1.041
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No