Crystallography Open Database

Information card for entry 4084336

Preview

Coordinates	4084336.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C44 H39 Co F10 P4
Calculated formula	C44 H39 Co F10 P4
Title of publication	Peripheral Methyl Activation in η4-1,2,3,4-Tetramethylcyclobutadienylcobalt Complexes: Template Synthesis and Subsequent Reactivity of Triphosphamacrocycles
Authors of publication	Edwards, Peter G.; Kariuki, Benson M.; Newman, Paul D.; Zhang, Wenjian
Journal of publication	Organometallics
Year of publication	2014
Journal volume	33
Journal issue	19
Pages of publication	5440
a	10.9766 ± 0.0002 Å
b	13.7217 ± 0.0003 Å
c	13.8448 ± 0.0003 Å
α	84.052 ± 0.001°
β	75.647 ± 0.001°
γ	79.706 ± 0.001°
Cell volume	1983.81 ± 0.07 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0794
Residual factor for significantly intense reflections	0.0467
Weighted residual factors for significantly intense reflections	0.0972
Weighted residual factors for all reflections included in the refinement	0.1093
Goodness-of-fit parameter for all reflections included in the refinement	1.05
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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