Information card for entry 4085216

Structure parameters

• Common name: 11 in manuscript
• Formula: C59 H61 B2 Cl2 F28 N2 P2 Rh
• Calculated formula: C59 H61 B2 Cl2 F28 N2 P2 Rh
• Title of publication: 1,2-Bis(di-tert-butylphosphino)imidazole (dtbpi): A Versatile Imidazole-Based, Rigid, Bulky Bisphosphine Ligand for Transition Metals
• Authors of publication: Brill, Marcel; Rominger, Frank; Hofmann, Peter
• Journal of publication: Organometallics
• Year of publication: 2015
• Journal volume: 34
• Journal issue: 2
• Pages of publication: 506
• a: 10.3228 ± 0.0007 Å
• b: 17.8177 ± 0.0012 Å
• c: 19.0426 ± 0.0013 Å
• α: 73.531 ± 0.0011°
• β: 83.6745 ± 0.0011°
• γ: 80.2522 ± 0.0011°
• Cell volume: 3303.1 ± 0.4 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0623
• Residual factor for significantly intense reflections: 0.0459
• Weighted residual factors for significantly intense reflections: 0.1054
• Weighted residual factors for all reflections included in the refinement: 0.1155
• Goodness-of-fit parameter for all reflections included in the refinement: 1.023
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No